The Preparatory Manual of Explosives: Radical, Extreme, Experimental, Explosives Chemistry Vol.1: A Comprehensive Look at a Variety of Radical Explosi, Paperback/Jared Ledgard

Descriere

Description The Preparatory Manual of Explosives: Radical, Extreme, Experimental Explosives Chemistry Vol. 1 is broken down into Section 1: a) Introduction; b) Dual bonding; c) The Element Nitrogen; d) The element oxygen; e) The element chlorine; f) Introduction to filtration; 1) Gravity filtration; a) Fluting Filter Paper for use in gravity filtration; 2) Vacuum Filtration (suction filtration); a) General Laboratory Techniques: Methods of heating; 1) Free flame; 2) Steam bath, or water bath; 3) Oil bath; 4) Electric Heating Mantles; 5) Hot Plates; a) Methods of Cooling; 1) Cold water bath; 2) Ice water bath; 3) Standard ice bath; 4) Salt/ice bath; 5) Dry ice/acetone bath; a) Cooling tricks of the trade; b) Recrystallization, and solid product recovery; c) Recrystallization; 1) General recrystallization utilizing heat only; a) Working example of recrystallization using heat only; 2) Recrystallization using seed crystals; 3) Recovering the product through low heat and vacuum; a) Washing liquids; b) Washing solids using non-vacuum techniques; c) Washing solids using vacuum techniques; d) Drying solids; e) Drying liquids to remove water; f) Laboratory safety; g) Laboratory glassware; h) Laboratory equipment; Section 2: Intermediates, Reagents, and Solvents; Section 3: Experimental Explosives Chemistry; Theoretical Preparation 1: 1, 3,5-trinitrohexazinane; Azinane; Theoretical Preparation 2: trisodium hexazinane-1, 3,5-triide; SOD; Theoretical Preparation 3: 3, 3',3''-hexazinane-1, 3,5-triyltris(triaza-1, 2-dien-2-ium-1-ide); HEXAAZIDE; HTA; Theoretical Preparation 4: diammonium trioxidane-1, 3-diide; diammonium trioxide; DATD; Theoretical Preparation 5: 3, 3'-trioxidane-1, 3-diylbis(triaza-1, 2-dien-2-ium-1-ide); TDTD; Theoretical Preparation 6: benzene-1, 3,5-triyltris(chlorane) nonaoxide; BTCN; Chlorane; Theoretical Preparation 7: 2, 4,6-trinitro-1, 3,5, 2,4, 6-trioxatriazinane; TNTOTA; oxatriazinane; Theoretical Preparation 8: (2, 4,6-trinitrobenzene-1, 3,5-triyl) tris(chlorane) nonao